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时间:2021年07月12日 来源:

力可OHN736&836系列仪器采用惰性熔融法,提供各种无机材料、钢铁、有色金属、硬质合金陶瓷材料中宽范围的氧氮氢同时测定。ONH836仪器通过***采纳客户的反馈意见和创新设计,力可***仪器采用触摸屏技术和在线软件平台,增强了仪器的可操作性,降低了分析成本,节省实验室桌面空间。


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力可**的Cornerstone碳硫分析软件采用触摸屏界面使用户可完整的达到分析控制、方法设定、在线诊断、数据报告。Cornerstone碳硫分析软件允许用户在单一分析界面中完成日常的所有工作,快速而且简单易用。力可创新的批次和重复样品数据分组功能极大简化了样品结果输出和结果标准偏差的自动计算。减少了繁琐的额外数据处理。


Cornerstone氧氮氢分析软件同时支持***的数据文档格式和可变的报告格式。山东分析仪咨询报价

山东分析仪咨询报价,分析仪

Procedure – Powder/Chip Samples

Prepare the instrument as outlined in the operator's instruction manual.


Determine the instrument blank.

Login a minimum of three Blank reps.

Press the Analyze button on the instrument screen. After a short delay, the loading head slide-block will open. Insert a *** Nickel Capsule (leave capsule open) into the open port at top of loading head.

Note: samples using automation should be placed in the appropriate autoloader position before starting the analysis sequence. Once the sequence has started, the automatic analysis will start and end automatically.


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山东分析仪咨询报价,分析仪

Oxygen, Nitrogen, and Hydrogen in Refractory Metals

Summary

Oxygen and nitrogen are alloying elements in titanium, and are also classified as alpha stabilizing elements as they promote alpha phase alloys. Interstitial oxygen and nitrogen levels can be used to regulate the tensile strength of the material, but due to its high solubility can cause unwanted surface embrittlement. This phenomenon can be leveraged,however, under controlled processing to create surface films that increase surface hardness and wear properties.

Procedure – Powder/Chip Samples

Determine the instrument blank.


Press the Analyze button on the instrument screen, the lower electrode will close and the analysis sequence will start and end automatically.


Repeat steps 2b through 2g a minimum of three times.


Set the blank following the procedure outlined in the operator's instruction manual.


Instrument calibration/drift correction.

Login a minimum of three Standard reps.


Weigh approximately *** grams of a calibration/drift standard into a *** Nickel Capsule; enter the mass and standard identification into appropriate rep fields. If applicable, place the nickel capsule in the appropriate autoloader position.


Note: LECO Reference Materia***o not require preparation. See preparation statement on the reference material certificate. Solid Standards may be used to calibrate when chip or powder standards are not available.




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山东分析仪咨询报价,分析仪

Oxygen, Nitrogen, and Hydrogen in Refractory Metals

Summary

One of the most critical chemical specifications of titanium alloys is the hydrogen content. Too high of a

hydrogen content can cause hydrides to precipitate, which can lead to embrittlement and subsequent

cracking when the alloy is stressed. Hydrogen pickup typically occurs during downstream processing steps

such as heat treating, pickling, and cleaning.

The LECO ONH836 is a simultaneous oxygen, nitrogen, and hydrogen determinator that utilizes an electrode furnace, inert carrier gas, and both infrared and thermal conductivity detection to meet the analytical needs of the refractory metal industry. 

This application note was written specifically for use with the LECO ONH836 series determinator.


减少了繁琐的额外数据处理。山东分析仪咨询报价

可选六轴可旋转触摸屏幕,增强了操作的工效和直观性。山东分析仪咨询报价

氧氮氢分析仪的原理:分析样品在惰性气流存在下于石墨坩埚中加热熔融,其中脉冲炉温度可自由设定,并通过一个非接触式的光学温度传感器进行实时监控,用于实现样品的完全分解,反应所生成的CO H2和N2被带入到具有高稳定性和灵敏度的检测系统进行检测。对于CO的检测采用的是非色散性红外检测器,对于N2和H2的检测则采用热导检测器。

氧氮氢分析仪的特点:快速准确分析,自动化操作;精密气体校准;CO红外检测器,高分辨率和重现性的N、H热导池检测器;同一台仪器实现熔融提取和热提取;热提取分析时间可调;可自由选择温度*高达2500 °C;光学温度计温度测定和控制;所有检测器自动调零/自动水平控制(ALC);数据评估的自动优化选择范围;炉自动清洁和坩埚自动进样(可选);外设电脑进行操作和控制;样品信息保存; 所有样品数据可追踪查询;通过FTP或本地局域网进行数据传输; ON,H分析轻松切换。


山东分析仪咨询报价

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